A Comparative Study of the Reactions of Nitrosophenol And N Chloroquinonimine Wi
A Comparative Study of the Reactions of Nitrosophenol And N Chloroquinonimine Wi
C E Carleton Edgar Curran
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1. 19), diluted with 600 cc. Of distilled water, were added to the reaction mixture at the rate of about thirty drops per minute, the stirring being continued. The mixture first became 1 Baeyer and Caro, Ber. 7, 963. (1874). 19 black and tarry and later assumed a reddish tinge. After about the fifth hour of the addition of acid small crystals could be ; seen in the solution . After all . The acid was added the. Stirring was continued for six hours at the same temperature. Six hundred grams of c...ommon salt were then added and the mixture stirred two hours longer, the temperature being maintained at 6 to 10. The solid product was filtered onto a Buchner funnel and dried on a porous plate in air. The crude product is dark red and decomposes slowly on standing in air but quite suddenly when heated between 110 and 125C. PREPARATION OF NITROSOPHENOL-SODIUM SALT Crude nitrosophenol was purified by preparing the sodium salt and acidifying a solution of this substance when the pure product was desired.
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