A Comparative Study of the Reactions of Nitrosophenol And N Chloroquinonimine Wi

Cover A Comparative Study of the Reactions of Nitrosophenol And N Chloroquinonimine Wi
A Comparative Study of the Reactions of Nitrosophenol And N Chloroquinonimine Wi
C E Carleton Edgar Curran
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1. 19), diluted with 600 cc. Of distilled water, were added to the reaction mixture at the rate of about thirty drops per minute, the stirring being continued. The mixture first became 1 Baeyer and Caro, Ber. 7, 963. (1874).
19 black and tarry and later assumed a reddish tinge. After about the fifth hour of the addition of acid small crystals could be ; seen in the solution . After all . The acid was added the. Stirring was continued for six hours at the same temperature. Six hundred grams of c
...ommon salt were then added and the mixture stirred two hours longer, the temperature being maintained at 6 to 10. The solid product was filtered onto a Buchner funnel and dried on a porous plate in air.
The crude product is dark red and decomposes slowly on standing in air but quite suddenly when heated between 110 and 125C.
PREPARATION OF NITROSOPHENOL-SODIUM SALT Crude nitrosophenol was purified by preparing the sodium salt and acidifying a solution of this substance when the pure product was desired.


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