A Laboratory Manual Containing Directions for a Course of Experiments in Organic
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Evaporate the combined filtrates to crystallization and save a specimen of the lead salt. Heat the third portion until saturated with freshly precipitated copper hydroxide (obtained by precipitating a solution of copper sulphate with caustic soda solution and washing the precipitate thoroughly with water), filter, evaporate the filtrate to crystallization, and save a specimen of the copper salt.
With the 25 cc. Of the distillate perform the following experiments: (a) Heat a small quantity with ...some mercuric oxide and note the result. Explain. 42 (6) Heat some with a solution of silver nitrate and de- scribe and explain what takes place. (Explain why these two reactions are characteristic of formic acid. ) How is formic acid made from chloroform? Describe both the physical and chemical properties of the acid and all the salts made; save specimens of all the salts and of the distillate.
(Use the material in the bottle marked "Glycerol Residues" to start with, if it is available, instead of glycerol itself, and add only 50 grams of oxalic acid at a time.
What to read after A Laboratory Manual Containing Directions for a Course of Experiments in Organic?
You can find similar books in the "Read Also" column, or choose other free books by Orndorff, W. R. (William Ridgely), 1862-1927 to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
Evaporate the combined filtrates to crystallization and save a specimen of the lead salt. Heat the third portion until saturated with freshly precipitated copper hydroxide (obtained by precipitating a solution of copper sulphate with caustic soda solution and washing the precipitate thoroughly with water), filter, evaporate the filtrate to crystallization, and save a specimen of the copper salt.
With the 25 cc. Of the distillate perform the following experiments: (a) Heat a small quantity with ...some mercuric oxide and note the result. Explain. 42 (6) Heat some with a solution of silver nitrate and de- scribe and explain what takes place. (Explain why these two reactions are characteristic of formic acid. ) How is formic acid made from chloroform? Describe both the physical and chemical properties of the acid and all the salts made; save specimens of all the salts and of the distillate.
(Use the material in the bottle marked "Glycerol Residues" to start with, if it is available, instead of glycerol itself, and add only 50 grams of oxalic acid at a time.
What to read after A Laboratory Manual Containing Directions for a Course of Experiments in Organic?
You can find similar books in the "Read Also" column, or choose other free books by Orndorff, W. R. (William Ridgely), 1862-1927 to read onlineMoreLess
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