A Manual of Inorganic Chemistry, Arranged to Facilitate the Experimental Demonstration of the Facts And Principles of the Science

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2. When sulphydric acid gas is passed into an acidulated solution of an antimony-salt (that of tartar- emetic for example), a bright orange-red precipitate of a hydrated tersulphide of antimony is formed, which may be rendered anhy- drous at a moderate heat without losing its red color.
H.rp. 142. — Dissolve 2 grms. of tartar emetic in 50 c. c. of water and add to the solution a few drops of acetic acid ; pass a slow current of sulphuretted hydrogen, from a self-regulating generator (Appendix,
...§ 19), through this solution for ten minutes. The precipitate is the hydrated tersulphide of antimony. Collect this precipitate upon a filter and wash it.
l^xp. 143. — Pour a dilute cold'solution of caustic soda upon the washed precipitate of the last experiment as it lies upon the filter, and collect the filtrate in a test-tube ; if the whole precipitate does not shortly redissolve, pour the filtrate a second time upon the undissolved precipitate in the filter, or use an additional quantity of soda-lye, if necessary.


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