A Manual of Microchemical Analysis

Cover A Manual of Microchemical Analysis
A Manual of Microchemical Analysis
Judd, John W. (John Wesley), 1840-1916
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The insoluble carbonate is immersed in a drop of water, covered, and brought into full view under a low power of the microscope.
Close to the cover glass a drop of acid is placed, and on the opposite side a strip of dry filtering-paper, which starts the reaction by absorbing the water. Under this form the test has come into universal use for examining specimens of rocks. More delicacy and a more exact localisation of the bubbles is gained by spreading a thin layer of a mixture of gelatine and g
...lycerine over the sample. The reaction is started by spreading over this a second layer, acidulated with nitric or hydrochloric acid.
§ 41. Boron a. Precipitation as potassium fluoborate. Limit: 0.2 /xgr. of B. 1 b. Sublimation with ammonium fluosilicate. Limit : 0.4 /Agr. of B.
a. Dissolve in hydrofluoric acid or in hydrochloric acid 1 Behrens, Mikr. Meth. p. 38.
i REACTIONS 103 and ammonium fluoride and add potassium chloride or nitre. Dilute solutions must be concentrated. They will then yield better crystals than the thin, pale rhombs, hexagons, and A?


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