A Practical Treatise of Chemical Analysis, Including Tables for Calculations in Analysis
A Practical Treatise of Chemical Analysis, Including Tables for Calculations in Analysis
Heinrich Rose
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This being done, the liquor which is suspected to contain arsenic is gradually poured through the funnel h ; if this liquor be alkaline, it must first be rendered acid. When the liquor contains much organic matter, as when, for example, a stomach has been boiled in solution of potash, and the decoction has been rendered acid, not by nitric acid, but by muriatic or sulphuric acid, it is important to pour it in only by degrees, and by very small quantities at a time, because the disen- gagement o...f hydrogen gas produces a viscid froth which might ascend in the tube containing the chloride of calcium, especially if the flask be not very large. If the liquid really contains > It IB necessary, before kindling the gas or patting the spirit-lamp under the tabe, to wait until the disengagement of the hydrogen gas has proceeded for some ccmsider- able time, in order to make certain that all the atmospheric air has been expelled £rom the apparatus, else an explosion might take place. It is then absohUely requisite to ascertain that neither the zinc nor the acid employed contains arsenic.
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