A Systematic Handbook of Volumetric Analysis; Or, the Quantitative Estimation of Chemical Substances By Measure, Applied to Liquids, Solids, And Gases, Adapted to the Requirements of Pure Chemical Research, Pathological Chemistry, Pharmacy, Metallurgy, Ma

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of solid sodium hydrate in a liter of distilled water ; when cold, put it in a tall glass cylinder, and introduce about 100 sq. cm. of aluminium foil, which must be kept at the bottom of the solution by means of a glass rod. When the aluminium is dissolved, boil the solution briskly in a porcelain basin until about one-third of its volume has been evaporated, allow to cool, and make up to its original volume with water free from ammonia. The absence of nitrates is thus ensured.
(f) Broken pumic
...e. — Clean pumice is broken in pieces of the size of small peas, sifted free from dust, heated to redness for about an hour, and kept in a closely stoppered bottle.
(ij) Hydrochloric acid free from ammonia. — If the ordinary pure acid is not free from ammonia, it should be rectified from sulphuric acid. As only two or three drops are used in each experiment, it wiU be sufficient if that quantity does not contain an appreciable pro- portion of ammonia.
For the Estimation of Nitrites by G-riess's Process.


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