A Text book of Volumetric Analysis With Special Reference to the Volumetric Pro

Cover A Text book of Volumetric Analysis With Special Reference to the Volumetric Pro
A Text book of Volumetric Analysis With Special Reference to the Volumetric Pro
Henry W Henry William Schimpf
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(212 F. ) to a constant weight.
This residue should not weigh less than 0. 02 gm. Nor more than 0. 0224 gm. , corresponding to not less than 0. 9 nor more than i per cent, of strychnine.
. 0224 X IQO _, 2. 24 ESTIMATION OF THE IRON.
The aqueous liquid from which the strychnine has been removed in the manner described above, is heated on a water-bath until the chloroform and ammonia are entirely volatilized. This is then allowed to cool, and diluted with water to the volume of 100 cc. 25 cc. Of
...I Q2 A TEXT-BOOK OF VOLUMETRIC ANALYSIS.
this are transferred to a glass-stoppered bottle (having a capacity of 100 cc. ), 2 gms. Of hydrochloric acid and I gm. Of potassium iodide are then added, and the mix- ture kept at a temperature of 40 C. (104 F. ) for half an hour. After it has been allowed to cool add a few drops of starch T. S. , and titrate with decinormal so- dium thiosulphate V. S. Until the blue or greenish color N of the liquid is entirely discharged. 16 cc. Of the V. S. Should be required to produce this result, each cc.


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