Addition Compound Formation in Aqueous Solutions Hydrates At the Boiling Point
Addition Compound Formation in Aqueous Solutions Hydrates At the Boiling Point
Horatio Wales
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The boiling-point tubes used in this investigation were a modification of the usual Beckmann type, being slightly larger and with the arms placed near the top in order to give as small a vapor space as possible. Previous investigators have used gar- nets in the boiling point tubes to secure a uniform ebullition. We found that these were appreciably soluble in the boiling solu- iNernst, Theoretical Chemistry. 2Biltz, Zeit. Phys. Chem. 40, 207, (1902). tions of the stronger acids used, such as ox...alic and phosphoric acids, and substituted small quartz crystals with good results. The same weight, thirty grams, of quartz was always used in order to keep their volume^ constant. The boiling-point tube was connected to a large water man- ometer through an air reservoir (see diagram), by means of which the pressure on the liquid was kept constant at 760 milli- meters of mercury throughout each determination. The heater and the boiling-point tube were entirely surrounded with asbestos boards which served to prevent sudden cooling of the liquid by air currents and thus prevent sudden changes in the ther- mometer readings.
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