Adulterated Drugs And Chemicals

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Adulterated Drugs And Chemicals
Lyman F Lyman Frederic Kebler
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9 Soluble in 2 volumes; insoluble in more.
a Per rent of ester calculated as geranyl acetate.
The acid number was determined by dissolving a given weight of the oil in strong alcohol, in which aH the oils were soluble in all pro- portions, and titrating with decinormal alcoholic potash, at the ordi- nary temperature, using phenolphthalein as indicator. The figures Bul. Soc. Chim. , 1900 (3), 28: 37.
KOSE GERANIUM OIL AND ITS SUBSTITUTES. 25 indicate the number of milligrams of potassium hydroxi
...d required to neutralize the acidity of one gram of oil. The esters were esti- mated by adding an excess of alcoholic potash to the above solution, heating to boiling with a reflux condenser for about one hour, thru titrating back the excess of alkali by means of decinormal acid. From the amount of alkali consumed the necessary calculations can readily be made, either as geranyl tiglinate (C 10 H 17 CO 2 C 4 H 7 ) or geranyl acetate (C 10 H 17 CO 2 CH 3 ), as the case may require. The percentage of alcohol, free or combined, was determined by acetyliziug a given weight of oil with an equal amount of acetic anhydrid, in the presence of fused sodium acetate.

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