Agricultural Analysis a Manual of Quantitative Analysis for Students of Agricul

Cover Agricultural Analysis a Manual of Quantitative Analysis for Students of Agricul
Agricultural Analysis a Manual of Quantitative Analysis for Students of Agricul
Frank Thornton Addyman
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C. Of the seminormal acid from a burette (d, fig. 25) and set it on one side. Next weigh out accurately about -3 gram of pure dry urea. Place the iron tubes in the staple fixed in the drawer, just as the tube stands in fig. 25. By means of the copper funnel introduce sufficient of the soda lime and sugar mixture to fill an inch at the end of the tube. Pour as much granulated soda ° Fig. 26. Lime as could be held on a penny into the mortar. Turn out the urea on to this, and just cover it with fi...nely powdered soda lime. Then add about twice as much granulated soda lime as is already in the mortar, placing it first on the watch glass and pouring it thence into the mortar. This ensures that all the urea shall be re- moved from the glass. Now mix thoroughly with the steel spatula, and pour through the funnel into the tube. Rinse out the mortar with fresh granulated soda lime several times, pouring the rinsings into the tube, stopping when it is within 4 inches of the open end. Cover the soda lime with a plug of asbestos which fills about an inch of the tube when gently pressed down with a thick glass rod.

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