Analysis of Babbit

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Of water, filter and wash with hot water. Dilute filtrate to 150 c. C. With water and electrolyze with a current of A r Z7 100 =l to 1. 5 ampere and 2. 5 volts. Time, one to two hours. Temperature 50 to 60C. When all the metal is deposited, lower the beaker slowly (meantime continue the current), wash the cathode (serving as anode) and deposit with distilled water and immerse in 95% C 2 H 6 O for a few seconds. Dry in air bath at 160-19"0C. , to constant weight. Multiply the weight 64 ANALYSIS ...OF BABBITT of the deposit by a factor that has been found by direct experiment. 1 Weight taken . 5 gram.
1. 5 Used 3. 7 4 amperes ( =3. 75) and 3. 5 volts.
. 40 (Three 32 and three 16 c. P. Lamps in parallel). Time one hour.
Cylinder-f-deposit= 10. 2774 grams. = 10. 0400 " . 2374 gram.
. 2374 gram of Pb0 after 30 minutes at 160C. . 2369 " " " " 60 " " " . 2365 " " " " 90 " " " . 2363 " " " " 120 " " " . 2360 " " " " 150 " " " . 2369X. 8411 - X 100=39. 85% Pb.
. 5 gram.
K 2 Cr 2 O 7 Method. (Schwarz's method).


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