Analysses of Canned Peas And Beans Showing Composition of Different Grades

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Transfer 15 grams of the sample to a 500 cc Erlen- meyer flask with 200 cc of water; add 20 cc of hydrochloric acid (specific gravity 1. 125) and heat the solution to boiling for two and one-half hours with a reflux condenser. After nearly neutral- izing the acid with sodium hydroxid, transfer the solution to a 300 cc flask, add 5 cc of basic lead acetate, and complete the volume to the mark. Filter and remove the lead from a portion of the filtrate with a dry mixture of potassium sulphate and ...potassium carbonate. In the filtrate obtained from this treatment determine reducing sugar, using Munson and Walker's tables, and multiplying dextrose by 0. 9 to obtain starch.
Nitrogen. Determine nitrogen in 10 grams of sample by the Gunning method.
Ether extract. Extract the residue from the water determination for sixteen hours with ether.
aU. S. T>ept. Agr. , Bureau of Chemistry Bui. 107, Revised, p. 243. [Cir. 54] Crude fiber. Treat 20 grams of the sample according to the offi- cial method, " except that about 100 cc of hot water are added after each period of boiling and before filtering.


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