Deposition, Corrosion And Coloration of Tungsten Trioxide Electrochromic Thin Films

Cover Deposition, Corrosion And Coloration of Tungsten Trioxide Electrochromic Thin Films
Deposition, Corrosion And Coloration of Tungsten Trioxide Electrochromic Thin Films
Sun, Sey-Shing
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films have been confirmed to be amorphous, oxygen deficient (0/W = 2.76), and porous (>80% of bulk density).
2. X-ray photoelectron spectroscopy data have confirmed that the tungsten atoms in the as-deposited films existed not only as W , but also as W and W . The total concentration of subvalence states can be ^40% or higher.
3. The tungsten atoms in the as-deposited films are postulated to be present as WO , WO and WO according to their valence states.
The films structure can be visualized as
... a random network composed of WO and lower valent oxide molecules linking with each other through corner sharing oxygen bond.
4. The Pourbaix diagram for W indicates that WO is the thermo- dynamically stable specie for WO films stored in the acid 01 electrolyte (pH = 0.5, E = 0.4 V ), while W0 2 and W ? 0_ are not.
The conversion of WO and W ? into WO were observed as dissolu- tion of WO adn WO in acid to form crystalline WO. and its hydrates (i.e., WO.. HO and W0..2H 0). The reactions are 2+ uncertain, but appear to involve the formation of WO ions in solution and saturation of these solution.


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