Experimental Chemistry for Junior Students volume 1

Cover Experimental Chemistry for Junior Students volume 1
Experimental Chemistry for Junior Students volume 1
James Emerson Reynolds
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EXPERIMENTAL DETERMINATION OF THE VOLUME OCCUPIED BY ONE CENTIGRAM OF HYDROGEN.
WE have already learned from Experiment 18 that i centigram weight of hydrogen gas is evolved from acidulated water during the solution of 12-2 c. Grs. Of pure metallic magnesium; we, therefore, know how to get our unit weight of hydrogen. In the experi- ment cited we allowed the gas to escape: we shall now collect the gas and measure it.
Experiment 54. Obtain a tube about 40 c. Ms. Long and 2 c. Ms. Internal diamet
...er, graduated into 130 cubic centimeter divisions, a, fig. 39. Dilute 50 c. Cs. Of oil of vitriol with about a liter of water in a jug, and throw into the liquid a few scraps of metallic zinc. Hydrogen will be developed and the liquid will have nearly or quite satu- rated itself with the gas in a few minutes. Next pour some of the diluted acid into a tall narrow beaker b y and, having filled the graduated tube FIG. 39.
96 Introduction to Experimental Chemistry.
completely with the same liquid, invert it in the acid in the beaker and support it as shown.


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