Introduction to Chemical Technical Analysis

Cover Introduction to Chemical Technical Analysis
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Lately, however, hard potash soaps (Schicht's patent) have appeared. For many industrial purposes, substances such as rosin (rosin soaps), borax, water-glass, sodium alumin- ate, soda (to increase alkalinity), are added to soaps. Further- more, adulterants, such as chalk, heavy spar, starch, clay, etc. , etc. , are frequently encountered.
Analysis of Pure Soaps.
These may contain, beside the alkali salts of fatty acids, free alkali, alkaline carbonates, free fatty acids and neutral fats. * In a
...d- dition, a considerable quantity of water is always present.
(a) Water. About 5 grs. Of soap, removed from the center, in form of shavings, are dried at 50 for 1-2 hours. The temper- ature is then gradually raised to 100-110 and the soap is dried to constant weight.
Soft soaps are placed in a 100 c. C. Beaker containing a small gl^ss rod, and the bottom of which is covered 1. 3 cm. Deep with ignited quartz sand. Beaker + sand + rod are weighed, f About 5 grs. Soap are added and the whole is reweighed.


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