Introduction to the Preparation of Organic Compounds

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The conversion is accompanied by a change of colour from black to light grey. It is complete when no more steam is evolved. The tube is then heated to 180-190 in a suitable furnace (e. G. A Volhard petroleum furnace, fig. 15), and a slow stream of dry hydrogen is led through, trockener WasserstoK FIG. 15.
which on the way has passed through a vessel containing about 30 c. C. Of benzene. The hexa- hydrobenzene formed condenses in the ice- cooled receiver. The stream of hydrogen should not exceed
... 100 c. C. Per minute. In order to shorten the operation, the benzene may be warmed to 30. After about 7 hours the process is stopped. The benzene which has not been volatilised is weighed, and the ORGANIC COMPOUNDS 71 distillate, which contains some benzene, is treated with a nitrating mixture of sulphuric and nitric acids. The oil is separated from the heavier acid, washed with water, and dried over calcium chloride. On fractionating, hexa- hydrobenzene passes over at 80-82.
Yield at least 80 % of the benzene volatilised.


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