Laboratory Exercises to Accompany First Principles of Chemistry
Laboratory Exercises to Accompany First Principles of Chemistry
Raymond Bedell Brownlee
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; ring-stand with ring ; bunsen burner; two glass stirring rods; thermometer; pipette, lOcc. ; bal- ance with weights ; graduate, 100 cc. MATERIAL. Two pieces of cotton cloth (cheesecloth) weighing 5 g. Each ; two skeins white woolen yarn weighing 5 g. Each ; stock solution of Biebrich scarlet, tartrazine, or acid blue containing 5 g. To the liter (dissolve the color in hot water) ; stock solution of Glauber's salt (cryst. Sodium sulphate) containing 50 g. To the liter ; stock* solution of sulp...huric acid made by dissolving 55 cc. Of sulphuric acid (sp. Gr. 1. 84) in water and diluting to 1 liter ; picric acid ; sodium carbonate ; Castile soap. (a) Prepare 5 g. Samples of cotton cloth and of woolen yarn for the dye bath by boiling the cotton in a dilute solution of sodium carbonate and the wool in a soap solution as directed in Experiment 72. (6) Dissolve 0. 1 g. Of picric acid in 300 cc. Of water in an agateware vessel. Warm to 60 C. And then add a sample of cotton cloth and one of woolen yarn.
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