Laboratory Work in Applied Chemistry, for Students in Domestic Science

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Determination of Ash, Principle of the Method. — The milk is treated with nitric acid to assist in the oxidation of the organic matter, then evapo- 35 rated to dryness and finally ignited to burn ofif the carbonaceous material. The residue is the mineral matter or ash.
Apparatus. — Thin porcelain dish, Bunsen burner, tripod, triangle, desiccator, balance and weights.
Details of Procedure. — Carefully weigh the porcelain dish to the nearest milligram. Transfer to it from a weighing bottle a quan
...tity of milk weighed accurately to centigrams (approxi- mately 20 grams). Add 6 c.c. of nitric acid and evaporate on the steam bath. When dry, place on the tripod and heat cau- tiously to dull redness until the residue is perfectly white. Cool in a desiccator and weigh to the nearest milligram.
Calculation of Result. — Per cent, ash = 100 (weight of ash) /(weight of milk).
5a. Determination of Fat (Babcock Method).
Principle of the Method. — When concentrated sulphuric acid is added to milk the emulsion is destroyed, the milk is curdled, the casein subsequently dissolved.


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