Mercuri Organic Derivatives I the Mercurization of Aromatic Amines And Its Rel
Mercuri Organic Derivatives I the Mercurization of Aromatic Amines And Its Rel
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62.
The compound is yellow and crystalline. It is soluble in acetone and in boiling alcohol. It melts at 215, with decomposition.
11 The position of the mercury in this compound was determined by the method of Dimroth. 26 The acetate was treated with two equivalents of a solution of potassium perbromide. The product was then extracted with ether and the extract purified from alcohol; m. P. 112-113. When mixed with 4-nitro-2, 6-dibromo-monomethylaniline, prepared by the method of Blanksma, 26 th...e melting point was not lowered. The use of only one molecule of the bromine in solution yielded no definite compound. Since the position could not be thus in dispute the dibromo derivative was therefore isolated.
/?-Nitro-0-Acetoxymercuri-mono-ethylaniline, (C 6 H 8 (l)N. H. C2H 5 (4)NO2(2)Hg. O2- C2H 3 ). This compound was prepared from -nitro-mono-ethylaniline, and was purified from the unchanged raw material by recrystallization from alcohol.
Analyses. Subs. , 0. 2641: dry N 2, 15. 7 cc. (24.
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To quickly assess the difficulty of the text, read a short excerpt:
62.
The compound is yellow and crystalline. It is soluble in acetone and in boiling alcohol. It melts at 215, with decomposition.
11 The position of the mercury in this compound was determined by the method of Dimroth. 26 The acetate was treated with two equivalents of a solution of potassium perbromide. The product was then extracted with ether and the extract purified from alcohol; m. P. 112-113. When mixed with 4-nitro-2, 6-dibromo-monomethylaniline, prepared by the method of Blanksma, 26 th...e melting point was not lowered. The use of only one molecule of the bromine in solution yielded no definite compound. Since the position could not be thus in dispute the dibromo derivative was therefore isolated.
/?-Nitro-0-Acetoxymercuri-mono-ethylaniline, (C 6 H 8 (l)N. H. C2H 5 (4)NO2(2)Hg. O2- C2H 3 ). This compound was prepared from -nitro-mono-ethylaniline, and was purified from the unchanged raw material by recrystallization from alcohol.
Analyses. Subs. , 0. 2641: dry N 2, 15. 7 cc. (24.
What to read after Mercuri Organic Derivatives I the Mercurization of Aromatic Amines And Its Rel?
You can find similar books in the "Read Also" column, or choose other free books by Isadore Meyer Jacobsohn to read onlineMoreLess
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