Microscopic Examination of Steel

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MACROSTRUCTURE.
Macrostructure is the appearance of the etched surface seen by the naked eye. Micros true ture, on the other hand, is that appearance of the etched surface seen under a microscope. The macrostructure often yields important evidence concerning the qualities of the metal. The structure is usually developed on 8 MICROSCOPIC EXAMINATION OF STEEL a roughly polished area of considerable size, or if it is possible to work only with small sections, it is recommended that the test bars b
...e rough-polished on two sides, at right angles to each other, before being turned into shape. The development of the structure is accomplished by etching the surface with a 6 per cent solution of iodine in alcohol or with an 8 per cent solution of copper ammonium chloride. The former should always be prepared immediately before use, as it keeps in good condition only a relatively short time. The copper ammonium chloride should be used only for those specimens which can be dipped into it, and the time of action should be approximately i minute.

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