Polymerization Studies of 4-Substituted-1, 2, 4-Triazoline-3, 5- Diones And Synthesis of Model Compounds Related to Triple Strand Polymers
Polymerization Studies of 4-Substituted-1, 2, 4-Triazoline-3, 5- Diones And Synthesis of Model Compounds Related to Triple Strand Polymers
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volumetric flask were dried overnight in an oven and then connected to a vacuum pump, flamed out, cooled in a desiccator and then stoppered with serum caps.
The PhTD was transferred to the polymer tube in a nitrogen flushed glove bag. The DVE was added in the usual manner by means of a syringe. The monomer charge was 0.500 g. (2.85 mmol.) cf PhTD and 0.197 g. (2.31 mmol.) of DVE. After the customary freeze-thaw cycle on the high vacuum mani- fold the tube was sealed. The reaction was continued ...for 24 hours and 0.602 g. (86% yield) of product was obtained. The infrared absorbancej of the copolymer were identical to those of other 60° DVE-PhTD copolymers.
On dissolving for the molecular weight determination, an acetone soluble fraction (0.422 g.) and an acetone insoluble fraction were obtained. The molecular weight of the soluble fraction was determined to be 2540.
DVE-PhTD co pol yme ri zation in the p res ence of a f ree radical inhibitor- In the usual manner for 60° copolymurizations , a polymer tube was charged with 0.499 g.
What to read after Polymerization Studies of 4-Substituted-1, 2, 4-Triazoline-3, 5- Diones And Synthesis of Model Compounds Related to Triple Strand Polymers?
You can find similar books in the "Read Also" column, or choose other free books by Turner, S. Richard to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
volumetric flask were dried overnight in an oven and then connected to a vacuum pump, flamed out, cooled in a desiccator and then stoppered with serum caps.
The PhTD was transferred to the polymer tube in a nitrogen flushed glove bag. The DVE was added in the usual manner by means of a syringe. The monomer charge was 0.500 g. (2.85 mmol.) cf PhTD and 0.197 g. (2.31 mmol.) of DVE. After the customary freeze-thaw cycle on the high vacuum mani- fold the tube was sealed. The reaction was continued ...for 24 hours and 0.602 g. (86% yield) of product was obtained. The infrared absorbancej of the copolymer were identical to those of other 60° DVE-PhTD copolymers.
On dissolving for the molecular weight determination, an acetone soluble fraction (0.422 g.) and an acetone insoluble fraction were obtained. The molecular weight of the soluble fraction was determined to be 2540.
DVE-PhTD co pol yme ri zation in the p res ence of a f ree radical inhibitor- In the usual manner for 60° copolymurizations , a polymer tube was charged with 0.499 g.
What to read after Polymerization Studies of 4-Substituted-1, 2, 4-Triazoline-3, 5- Diones And Synthesis of Model Compounds Related to Triple Strand Polymers?
You can find similar books in the "Read Also" column, or choose other free books by Turner, S. Richard to read onlineMoreLess
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