Practical Proofs of Chemical Laws: a Course of Experiments Upon the ...
Practical Proofs of Chemical Laws: a Course of Experiments Upon the ...
Vaughan Cornish
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— Preparation of the two chlorides of copper in a state of purity. Cuprous chloride, — (The pupil should be ac- quainted with the mode of formation of this salt.) Take the salt as obtained from the dealers (which is not pure), dissolve it in a little strong, pure hydrochloric acid, and pour the clear solution into a large beaker of distilled water. The cuprous chloride is thrown down as a white precipitate, which quickly settles to the bottom of the beaker. Syphon off the bluish solution as qui...ckly as pos- sible ; the loss of some of the precipitate does not matter. Fill the beaker again with distilled water, stir up, allow to settle, and syphon off again. Repeat the operation a third time, to ensure that the washings are free from cupric salt. The pure white cuprous chloride which remains at the bottom of the beaker would readily oxidise if dried. No attempt, therefore, is made to dry and weigh the substance, it being sufficient for our purpose to determine the ratio of copper to chlorine in an unknown weight of the salt.
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