Practical Test book of Chemistry

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(40 minims) cold water). Reduces also an ammoniacal silver solu- tion.
(5) A mixture of equal parts sugar and Picrotoxin is colored red by the addition of sulfuric acid (Reagent 21).
Test for Pilocarpin, CiiHi 6 N 2 O 2 .
Pilocarpin is an alkaloid found in jaborandi; the official salt is the hydrochlorate, and is in small, white crystals, odorless, and having a faintly bitter taste; deliquescent on exposure to damp air; very soluble in water and in alcohol; almost insoluble in ether or chlorofo
...rm. The aqueous solution (1 in 100) of the salt is neutral or has a faintly acid reaction upon litmus paper.
(1) A characteristic reaction, had in common with cocain, is that Pilocarpin reduces calomel to Hg (blackens it) when 0. 010 gm. (J gr. ) of the alkaloid or the hydro- chlorate and 1 gm. (15J grs. ) of mercurous chlorid are triturated together and moistened by the breath.
(2) Another reaction is the behavior of the precipitate obtained from Reagent 12 in a diluted solution of the hydrochlorate; the amorphous precipitate sinks to the bottom, in the course of a day, in oily drops.


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