Preparation And Deprotonation of Certain Pi-Arene-Pi-Cyclopentadienyliron(11) Salts
Preparation And Deprotonation of Certain Pi-Arene-Pi-Cyclopentadienyliron(11) Salts
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m.p. reported).
NMR (acetone-d,): cyclopentadienyl - 5.22 (s,5), coordinated arene - 6.47 (s,5), uncoordinated arene - 7.37 (s,5), methylene - 4.25 (s,2).
'If the product is not completely dry at this point, oiling will occur and good recrystal 1 ized product is almost impossible to obtain.
If dichloromethane is used to dissolve the salt, any water remaining is easily removed by using a separatory funnel. The use of dichloro- methane allows a more rapid work-up as it obviates the tedious step o...f completely drying out the product before recrystal 1 izat ion.
63 IR (KBr): 3128 (m) , 1603 (w) , 1532 (w) , IA98 (m) . 1^68 (m) , 1^58 (m) , lif25 (s), 8i»5 (vs, broad), 7^0 (5), 710 (s) , 559 (s) , '♦97 (s) , 477 (s) cm .
27 n^-Fluorene-n^-cycl open tad ienyl i ron(l I) Hexaf luorophosphate Ferrocene (8.0 g, 0.0't3 mol), fluorene (10.0 g, O.O603 mol), alumin- um chloride powder (11. 65 g, 0.0875 mol), aluminum powder (3.29 g, 0.122 a mol), and decahydronaphthalene {kO ml) were added to the reaction ves- sel and stirred at 155°C.
What to read after Preparation And Deprotonation of Certain Pi-Arene-Pi-Cyclopentadienyliron(11) Salts?
You can find similar books in the "Read Also" column, or choose other free books by Hendrickson, William Arthur to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
m.p. reported).
NMR (acetone-d,): cyclopentadienyl - 5.22 (s,5), coordinated arene - 6.47 (s,5), uncoordinated arene - 7.37 (s,5), methylene - 4.25 (s,2).
'If the product is not completely dry at this point, oiling will occur and good recrystal 1 ized product is almost impossible to obtain.
If dichloromethane is used to dissolve the salt, any water remaining is easily removed by using a separatory funnel. The use of dichloro- methane allows a more rapid work-up as it obviates the tedious step o...f completely drying out the product before recrystal 1 izat ion.
63 IR (KBr): 3128 (m) , 1603 (w) , 1532 (w) , IA98 (m) . 1^68 (m) , 1^58 (m) , lif25 (s), 8i»5 (vs, broad), 7^0 (5), 710 (s) , 559 (s) , '♦97 (s) , 477 (s) cm .
27 n^-Fluorene-n^-cycl open tad ienyl i ron(l I) Hexaf luorophosphate Ferrocene (8.0 g, 0.0't3 mol), fluorene (10.0 g, O.O603 mol), alumin- um chloride powder (11. 65 g, 0.0875 mol), aluminum powder (3.29 g, 0.122 a mol), and decahydronaphthalene {kO ml) were added to the reaction ves- sel and stirred at 155°C.
What to read after Preparation And Deprotonation of Certain Pi-Arene-Pi-Cyclopentadienyliron(11) Salts?
You can find similar books in the "Read Also" column, or choose other free books by Hendrickson, William Arthur to read onlineMoreLess
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