The book Qualitative Analysis for Secondary Schools was written by author Cyrus Wendell Irish Here you can read free online of Qualitative Analysis for Secondary Schools book, rate and share your impressions in comments. If you don't know what to write, just answer the question: Why is Qualitative Analysis for Secondary Schools a good or bad book?
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Add HC1. Pp. Yellow As 2 S 3 and As 2 S 5 (S#), As pres. Confirm by drying pp. , mixing with Na 2 C0 3 and KCN, and heating in bulb tube. Arsenic mirror on upper part of tube, As pres. Notes and Suggestions The precipitation of S, on addition of HC1, must not be mistaken for this group. Sulphur will precipitate, white, when HC1 is added to (NH 4 ) 2 S. This difficulty can be overcome in part by using small quantities of (NH 4 ) 2 S. When heating solution A with an iron nail, a precipitate may b...e due to carbon from the iron, or metallic Sb from the reducing action of nascent H, or particles of undissolved iron. In the case of the battery 48 BASIC ANALYSIS action in solution B, if enough Zn is used to neutralize all acid and the action is carried to completion, most of the Sn will be deposited with Sb on the Pt foil. The Sn may be dissolved off with HC1 and warm H 2 O as SnCl 2 . Sb is undissolved. This test for Sn serves as a check on the preceding test. The (NH 4 ) 2 CO 3 should not contain much NH 4 OH, as its presence will dissolve traces of SnS and Sb 2 S 3, and thus make necessary the confirmatory test for As, with Na 2 CO 8 and KCN.
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