Quantitative Metallurgical Analysis: Selected Methods for Chemical Analaysis ...

Cover Quantitative Metallurgical Analysis: Selected Methods for Chemical Analaysis ...
Quantitative Metallurgical Analysis: Selected Methods for Chemical Analaysis ...
Charles Frederick Sidener
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XVII, page 129.
Mixter & Du Bois, Jour. Am. Chem. 80c.. Vol. XIX, page 614.
H. C. Babbitt. Jour. Am. Chem. 80c., Vol. VII, page 165.
E. D. Campbell, Jour. Am. Chem. 80c., Vol. VII, page 2.
Dudley & Pease, Jour. Am. Chem. 80c., Vol. VII, page 519, P. W. Shimer, Jour. Am. Chem. 80c., Vol. XXI, page 723.
26 METALLURGICAL ANALYSIS Reduction of the MoOJn a Reductor: Obtain the yellow precipitate and dissolve it in ammonia just as described oti page 25 and the solution is allowed to run into a clean
...beaker. Wash the filter paper with water until the solution measures about 60-70 c.c. Add to the liquid in the beaker 10 c.c.
concentrated sulphuric acid and pass it through the reductor which has just been cleaned by passing through it distilled water and then 100 c.c. of warm dilute sulphuric acid, strength : 25 c.c. con- centrated sulphuric acid per liter of distilled water. After passing the molybdate solution through the reductor, wash with about 200 c.c. of the warm dilute sulphuric acid, and finally with about 50 c.c.


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