Reactions of Amine Boranes And Related Compounds: (I) Mechanism of Dehydrogenation of Dimethylamine Borane (Ii) Synthesis of Trimethylamine Chloroboranes
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88 89 The unsuccessful attempts to prepare (CH,)2DNBH, or (CH,)2HNBD2 with only the isotopic distribution indicated, suggested that before any experiments can be successfully designed for these compounds, more information about hydrogen-deuterium exchsmge reactions of boron-nitrogen compounds would be necessary. These exchange reactions, or merely the possibility of such, means that any experiments with isotopicsLlly labelled amine boranes must be examined critically to make sure that it is not... an exchange reaction which gave the measured results. In this work, the hydrogen elimination reaction of dimethylamine borane has been con- sidered in view of the possibility of an exchange reaction.
The evidence strongly inferred a bimolecular reaction.
SUMMARY To determine the mechanism of the dehydrogenation of dimethylamine borane, (CH^)2HNBH^, the following compounds were prepared, N-deuterodimethyl amine borane-d^, (CH:,)^DNBD,, N- deuterodimethylamine borane, (CH,)2DNBH, and dimethylamine borane-d^, (CH,)2HKBD^ were prepared by condensing together the appropriate isotopically labelled diborane and dimethyl- amine.
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To quickly assess the difficulty of the text, read a short excerpt:
88 89 The unsuccessful attempts to prepare (CH,)2DNBH, or (CH,)2HNBD2 with only the isotopic distribution indicated, suggested that before any experiments can be successfully designed for these compounds, more information about hydrogen-deuterium exchsmge reactions of boron-nitrogen compounds would be necessary. These exchange reactions, or merely the possibility of such, means that any experiments with isotopicsLlly labelled amine boranes must be examined critically to make sure that it is not... an exchange reaction which gave the measured results. In this work, the hydrogen elimination reaction of dimethylamine borane has been con- sidered in view of the possibility of an exchange reaction.
The evidence strongly inferred a bimolecular reaction.
SUMMARY To determine the mechanism of the dehydrogenation of dimethylamine borane, (CH^)2HNBH^, the following compounds were prepared, N-deuterodimethyl amine borane-d^, (CH:,)^DNBD,, N- deuterodimethylamine borane, (CH,)2DNBH, and dimethylamine borane-d^, (CH,)2HKBD^ were prepared by condensing together the appropriate isotopically labelled diborane and dimethyl- amine.
What to read after Reactions of Amine Boranes And Related Compounds: (I) Mechanism of Dehydrogenation of Dimethylamine Borane (Ii) Synthesis of Trimethylamine Chloroboranes?
You can find similar books in the "Read Also" column, or choose other free books by Wiggins, James William, 1940- to read onlineMoreLess
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