Scientific American Supplement, No. 362, December 9, 1882
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, to convert potassiumnitrate and chloride into the fixed sulphate. The sulphuric acid attacksthe manure energetically, and much facilitates the incineration, whichmay be effected at a dark red heat. The ignited portion (10 grms. ) isexhausted with boiling distilled water acidulated with hydrochloricacid, and the filtrate, when cold, is made up to 500 c. C. Of thissolution 50 c c. , representing 1 grm. Of the sample, are taken, and, after being heated until close upon ebullition, baryta-water i...s addeduntil a strong alkaline reaction is obtained. The sulphuric andphosphoric acids, alumina, magnesia, etc, are thus precipitated. Thefiltrate is heated to a boil, and mixed with ammonia and ammoniumcarbonate, to precipitate the excess of baryta in solution. The lasttraces of lime are eliminated by means of a few drops of ammoniumoxalate. The filtrate is evaporated down on the water-bath, and theammoniacal salts are expelled by carefully raising the temperature todull redness. After having taken up the residue in distilled water itis treated with platinum chloride, and the potassium chloro-platinateobtained is reduced with oxalic acid.
What to read after Scientific American Supplement, No. 362, December 9, 1882?
You can find similar books in the "Read Also" column, or choose other free books by Various to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
, to convert potassiumnitrate and chloride into the fixed sulphate. The sulphuric acid attacksthe manure energetically, and much facilitates the incineration, whichmay be effected at a dark red heat. The ignited portion (10 grms. ) isexhausted with boiling distilled water acidulated with hydrochloricacid, and the filtrate, when cold, is made up to 500 c. C. Of thissolution 50 c c. , representing 1 grm. Of the sample, are taken, and, after being heated until close upon ebullition, baryta-water i...s addeduntil a strong alkaline reaction is obtained. The sulphuric andphosphoric acids, alumina, magnesia, etc, are thus precipitated. Thefiltrate is heated to a boil, and mixed with ammonia and ammoniumcarbonate, to precipitate the excess of baryta in solution. The lasttraces of lime are eliminated by means of a few drops of ammoniumoxalate. The filtrate is evaporated down on the water-bath, and theammoniacal salts are expelled by carefully raising the temperature todull redness. After having taken up the residue in distilled water itis treated with platinum chloride, and the potassium chloro-platinateobtained is reduced with oxalic acid.
What to read after Scientific American Supplement, No. 362, December 9, 1882?
You can find similar books in the "Read Also" column, or choose other free books by Various to read onlineMoreLess
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