Study of the Production of Resorcin

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2. Acidification of the fusion to form resorcin.
3. Extraction of the resorcin.
4. Purification of the resorcin.
These experiments were undertaken with the idea of determining the most economical means of production.
1. Fusion of the sodium m-benzenedisulph- onate : The conversion of the disulphonate body into the diphenate body is accomplished by fusion with NaOH. There are two common ways of making this 21 fusionj first, in an open kettle; second, in an autoclave. The first is the one describ
...ed to the greatest extent in the literature. The second method of making a fusion in an autoclave is given in an article by A.H, Ney and D.J. Van Marie on "The Processes of the Organic Chemical Industry Used in the Manufacture of Intermediate Products", published in the Metallurgical and Chemical Engineering Magazine, February 15, 1917.
"Caustic fusion with water is carried out in autoclaves under pressure, v/hich allows the amount of caustic soda to be cut down materially and prevents oxidation.


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