Synthetic And Solvolytic Studies in the Bismethanonaphthalene System
Synthetic And Solvolytic Studies in the Bismethanonaphthalene System
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Anal.: Calcd. for C H 0.,: C, 70.55; H, 9.31 Found: C, 70.61; H f 9.32.
~) f. 9 7 Preparation of 12 , 12-dimethoxytetracyclo [6 . 2 . 1 . 1 ' .0 ' ]- dodec-11-yl p-bronobenzenesulfonate (55)-OBs A solution of 1.3 g (5.5 mmol.) of (55_) -OH and 3.0 g (12 mmol.) of p-bromobenzenesulf onyl chloride in 75 ml of 44 precooled pyridine was maintained at 10 °C for 24 hrs.
This solution was poured into 300 ml of ice/water and extracted with 2 x 250 ml of ether. The combined ether layers were Ill washed ...with 400 ml of 3 _N hydrochloric acid, dried with anhydrous magnesium sulfate, filtered, and the ether re- moved under vacuum to give essentially a quantitative yield of crude (_55)-OBs. Recrystallization from benzene gave white prisms, m. p. 200.5 - 202.5 °C. The infrared spectrum (KBr) contained the following absorption bands: 2850 (m) , 1570 (m) , 1350 (s), 1190 (s), 960 (s) , 880 (s) , and 740 (s) cm" 1 . The Hnmr spectrum (CDCl-J contained the following resonances: 6 7.76 (aa'bb' quartet, 4; aromatic); 5.2 8 (broad s, 1; H, , ) ; 3.20 (s, 6; OCH.) ; and 1.1 - 2.2 (m, 14).
What to read after Synthetic And Solvolytic Studies in the Bismethanonaphthalene System?
You can find similar books in the "Read Also" column, or choose other free books by Timberlake, John Foushee to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
Anal.: Calcd. for C H 0.,: C, 70.55; H, 9.31 Found: C, 70.61; H f 9.32.
~) f. 9 7 Preparation of 12 , 12-dimethoxytetracyclo [6 . 2 . 1 . 1 ' .0 ' ]- dodec-11-yl p-bronobenzenesulfonate (55)-OBs A solution of 1.3 g (5.5 mmol.) of (55_) -OH and 3.0 g (12 mmol.) of p-bromobenzenesulf onyl chloride in 75 ml of 44 precooled pyridine was maintained at 10 °C for 24 hrs.
This solution was poured into 300 ml of ice/water and extracted with 2 x 250 ml of ether. The combined ether layers were Ill washed ...with 400 ml of 3 _N hydrochloric acid, dried with anhydrous magnesium sulfate, filtered, and the ether re- moved under vacuum to give essentially a quantitative yield of crude (_55)-OBs. Recrystallization from benzene gave white prisms, m. p. 200.5 - 202.5 °C. The infrared spectrum (KBr) contained the following absorption bands: 2850 (m) , 1570 (m) , 1350 (s), 1190 (s), 960 (s) , 880 (s) , and 740 (s) cm" 1 . The Hnmr spectrum (CDCl-J contained the following resonances: 6 7.76 (aa'bb' quartet, 4; aromatic); 5.2 8 (broad s, 1; H, , ) ; 3.20 (s, 6; OCH.) ; and 1.1 - 2.2 (m, 14).
What to read after Synthetic And Solvolytic Studies in the Bismethanonaphthalene System?
You can find similar books in the "Read Also" column, or choose other free books by Timberlake, John Foushee to read onlineMoreLess
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