Synthetic And Solvolytic Studies in the Endo, Exo-Bismethanonapthalene [sic] System
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Synthetic And Solvolytic Studies in the Endo, Exo-Bismethanonapthalene [sic] System
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In our eReader you can find the full English version of the book. Read Synthetic And Solvolytic Studies in the Endo, Exo-Bismethanonapthalene [sic] System Online - link to read the book on full screen. Our eReader also allows you to upload and read Pdf, Txt, ePub and fb2 books. In the Mini eReder on the page below you can quickly view all pages of the book - Read Book Synthetic And Solvolytic Studies in the Endo, Exo-Bismethanonapthalene [sic] System
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2 . 1 . 1 ' .0 ' ] - dod ec- 4 - en- 11-yl-p-me thy 1 benzene sulfonate (69 ) -OTs A 0.124 gram (0.344 mmoles) sample of (69) -OTs was dissolved in 10 mL 0.02879 N sodium acetate in acetic acid containing 1% acetic anhydride. This mixture was placed in a volumetric flask, sealed and heated at 35°C for 35 hours. The flask was cooled to room temperature and the mixture poured into 100 mL of ice water. The aqueous mix- ture was extracted with 4 x 50 mL of pentane. The pentane extractions were comb...ined and washed with 2 x 50 mL of water, 2 x 50 mL of 10% aqueous sodium carbonate, and fi- nally 50 mL of water. The pentane phase was then dried over anhydrous potassium carbonate, filtered, and the pentane removed under reduced pressure to yield 0.058 grams of product. The infrared spectrum (NaCl, neat) contained only one carbonyl absorption at 1710 cm . The Hnmr spectrum reveals that the mixture contains approximately 85% of the acetate ( 7JL) -OAc and 15% of the corresponding tosylate (71^) -OAc.
What to read after Synthetic And Solvolytic Studies in the Endo, Exo-Bismethanonapthalene [sic] System?
You can find similar books in the "Read Also" column, or choose other free books by Wallace, Benjamin to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
2 . 1 . 1 ' .0 ' ] - dod ec- 4 - en- 11-yl-p-me thy 1 benzene sulfonate (69 ) -OTs A 0.124 gram (0.344 mmoles) sample of (69) -OTs was dissolved in 10 mL 0.02879 N sodium acetate in acetic acid containing 1% acetic anhydride. This mixture was placed in a volumetric flask, sealed and heated at 35°C for 35 hours. The flask was cooled to room temperature and the mixture poured into 100 mL of ice water. The aqueous mix- ture was extracted with 4 x 50 mL of pentane. The pentane extractions were comb...ined and washed with 2 x 50 mL of water, 2 x 50 mL of 10% aqueous sodium carbonate, and fi- nally 50 mL of water. The pentane phase was then dried over anhydrous potassium carbonate, filtered, and the pentane removed under reduced pressure to yield 0.058 grams of product. The infrared spectrum (NaCl, neat) contained only one carbonyl absorption at 1710 cm . The Hnmr spectrum reveals that the mixture contains approximately 85% of the acetate ( 7JL) -OAc and 15% of the corresponding tosylate (71^) -OAc.
What to read after Synthetic And Solvolytic Studies in the Endo, Exo-Bismethanonapthalene [sic] System?
You can find similar books in the "Read Also" column, or choose other free books by Wallace, Benjamin to read onlineMoreLess
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