Synthetic And Spectroscopic Studies of Metal Carboxylate Dimers
Synthetic And Spectroscopic Studies of Metal Carboxylate Dimers
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for Rh 2 C 12 H 18 N 2 8 : C, 27.50; H, 3.46; N, 5.34. Found: C, 27.54; H, 3.53; N, 5.02.
Bi s ( tri phenyl phosphi ne ) tetraki s ( tri f 1 uoroacetato )di rhodi um( 1 1 ) This complex was synthesized following the procedure of Cotton and co-workers. 111 Rh 2 (0 3 CCF 3 ) 4 (0.050 g, 0.076 mmol) was dissolved in methanol (5 mL). Triphenylphosphine (0.040 g, 0.15 mmol) was dissolved in hot methanol (~5 mL). This solution was added to the blue Rh 2 (0 2 CCF 3 ) 4 (CH 3 0H) 2 solution to give an ...immediate dark brown color.
119 The solution quickly became colorless and purplish brown needle crystals were deposited. Filtration and washing with methanol afforded 0.085 g (0.075 mmol, 942). Anal. Calcd. for Rh 2 C 44 H 30 P 2 F 12 8 : C, 44.66; H, 2.56; P, 5.23. Found: C, 44.18; H, 2.67; P, 5.18. Orange Rh 2 (but) 4 (PPh 3 ) 2 was synthesized in the same manner in 822 yield. Anal.
Calcd. for Rh 2 C 52 H 58 P 2 8 : C, 57.89; H, 5.43; P, 5.74. Found: C, 58.07; H, 5.40; P, 5.88.
Bis (tri phenyl phosphite)tetrakis(trifluoroacetato)dirhodium(II) Rh 2 (0 2 CCF 3 ) 4 (0.178 g, 0.286 mmol) was dissolved in methanol (10 mL).
What to read after Synthetic And Spectroscopic Studies of Metal Carboxylate Dimers?
You can find similar books in the "Read Also" column, or choose other free books by Telser, Joshua A. to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
for Rh 2 C 12 H 18 N 2 8 : C, 27.50; H, 3.46; N, 5.34. Found: C, 27.54; H, 3.53; N, 5.02.
Bi s ( tri phenyl phosphi ne ) tetraki s ( tri f 1 uoroacetato )di rhodi um( 1 1 ) This complex was synthesized following the procedure of Cotton and co-workers. 111 Rh 2 (0 3 CCF 3 ) 4 (0.050 g, 0.076 mmol) was dissolved in methanol (5 mL). Triphenylphosphine (0.040 g, 0.15 mmol) was dissolved in hot methanol (~5 mL). This solution was added to the blue Rh 2 (0 2 CCF 3 ) 4 (CH 3 0H) 2 solution to give an ...immediate dark brown color.
119 The solution quickly became colorless and purplish brown needle crystals were deposited. Filtration and washing with methanol afforded 0.085 g (0.075 mmol, 942). Anal. Calcd. for Rh 2 C 44 H 30 P 2 F 12 8 : C, 44.66; H, 2.56; P, 5.23. Found: C, 44.18; H, 2.67; P, 5.18. Orange Rh 2 (but) 4 (PPh 3 ) 2 was synthesized in the same manner in 822 yield. Anal.
Calcd. for Rh 2 C 52 H 58 P 2 8 : C, 57.89; H, 5.43; P, 5.74. Found: C, 58.07; H, 5.40; P, 5.88.
Bis (tri phenyl phosphite)tetrakis(trifluoroacetato)dirhodium(II) Rh 2 (0 2 CCF 3 ) 4 (0.178 g, 0.286 mmol) was dissolved in methanol (10 mL).
What to read after Synthetic And Spectroscopic Studies of Metal Carboxylate Dimers?
You can find similar books in the "Read Also" column, or choose other free books by Telser, Joshua A. to read onlineMoreLess
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