Synthetic Inorganic Chemistry a Course of Laboratory And Classroom Study for Fi
Synthetic Inorganic Chemistry a Course of Laboratory And Classroom Study for Fi
Arthur a Arthur Alphonzo Blanchard
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grape sugar, 100 grams. alcohol, 45 cc. Apparatus: 8-inch evaporating dish. 2-liter common bottle. suction filter. 350 cc. Casserole, 3 beakers, and 3 8-inch common filters. Procedure: Dissolve the blue vitriol and the Rochelle salt each in 200 cc. Of hot water, filter the solutions separately if they are not clear, and when they are nearly cold mix them together in the 8-inch dish. In the meantime dissolve the sodium hydroxide in 200 cc. Of water, cool it completely, filter if not clear, and p...our it in a thin stream into the mixture in the dish, stirring constantly and being careful not to allow the mixture to get more than barely warm from the reaction. A clear solution results, but one of so deep blue a color as to appear almost like ink. Dissolve the grape sugar in 150 cc. Of water, filter if necessary, add it to the solution in the dish, and boil the mixture until the copper has pre- cipitated as the bright red cuprous oxide, and the blue color has disappeared from the liquid. Transfer the contents of the dish to the 2-liter bottle, add water to fill the latter, mix the contents thoroughly, and let settle for about 15 minutes.
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