The Analysis of Coal With Phenol As a Solvent

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The Analysis of Coal With Phenol As a Solvent
Samuel Wilson Parr
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No PRE- VIOUS HEATING OF RESIDUE.
FIG. 33.
SAME AS IN FIG. 32. PREVIOUSLY HEATED go HOURS AT 105' FIG. 34.
SAME AS IN FIG. 32. PREVIOUSLY HEATED 242 HOURS AT 105' PARR-HADLEY ANALYSIS OF COAL WITH PHENOL AS A SOLVENT 2$ For purposes of comparison of the absorption rates of extract and residue, the above results were plotted. Plotting time against dimin- ished pressure in millimeters, it is seen that the rate of absorption was faster in the case of the residue.
g ury rs of I I inis 8 40 80 160 2
...00 140 IZO Hours.
FIG. 6. RATE OF ABSORPTION OF OXYGEN BY RESIDUE AND EXTRACT.
The results as given in Tables 12 and 13 show that oxygen was taken up by both the residue and extract. The amount of oxygen that ILLINOIS ENGINEERING EXPERIMENT STATION had been absorbed when the experiment was stopped was about 4-5 cc. In the case of the residue, and 2-2^ cc. In the case of the extract. The experiment does not show absolutely that oxidation had taken, place, but from our knowledge of coal we would be led to suspect that such was the case.


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