The Analysis of Non-Ferrous Alloys
The Analysis of Non-Ferrous Alloys
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anorg. Chem., 32 (1902), 362.
* Reifl, Berichte, xiv. 1172.
Digitized by VjOOQIC 84 THE ANALYSIS OF NON-FERROUS ALLOYS to be 812(0204)3 . K2C2O4), and to estimate the excess of potassium oxalate in an aliquot portion of the filtrate. It is not advisable to add any great excess of potassium oxalate in this method, and the solution should not contain any large excess of free acid — even acetic. The precipita- tion with potassium oxalate is quite complete and of the known composition, but not so w...ith either sodium or ammonium oxalate.
Other volumetric methods that have been suggested include the precipitation of the bismuth with an excess of potassium iodate, followed by the removal of the precipitate and the estimation of the excess of potassium iodate in the filtrate by the addition of potassium iodide, and the titra- tion of the Uberated iodine with sodium thiosulphate. This is stated to be unreliable by Rupp and Krauss,^ as the pre- cipitate is not pure bi8muthiodateBi(I03)3, but Bi(OH) (103)2.
What to read after The Analysis of Non-Ferrous Alloys?
You can find similar books in the "Read Also" column, or choose other free books by Ibbotson, Fred. [from Old Catalog] to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
anorg. Chem., 32 (1902), 362.
* Reifl, Berichte, xiv. 1172.
Digitized by VjOOQIC 84 THE ANALYSIS OF NON-FERROUS ALLOYS to be 812(0204)3 . K2C2O4), and to estimate the excess of potassium oxalate in an aliquot portion of the filtrate. It is not advisable to add any great excess of potassium oxalate in this method, and the solution should not contain any large excess of free acid — even acetic. The precipita- tion with potassium oxalate is quite complete and of the known composition, but not so w...ith either sodium or ammonium oxalate.
Other volumetric methods that have been suggested include the precipitation of the bismuth with an excess of potassium iodate, followed by the removal of the precipitate and the estimation of the excess of potassium iodate in the filtrate by the addition of potassium iodide, and the titra- tion of the Uberated iodine with sodium thiosulphate. This is stated to be unreliable by Rupp and Krauss,^ as the pre- cipitate is not pure bi8muthiodateBi(I03)3, but Bi(OH) (103)2.
What to read after The Analysis of Non-Ferrous Alloys?
You can find similar books in the "Read Also" column, or choose other free books by Ibbotson, Fred. [from Old Catalog] to read onlineMoreLess
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