The Analysis of Non Ferrous Alloys
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1 The same end is secured by some workers by the addition of alcohol, though this might result in the pre- cipitation of magnesium salts if used too liberally. Rose recommended its addition to the extent of one-fourth the volume of the solution. Others make use of a correction for the solubility of the precipitate. Puller, 2 for example, adds to the weightf of MgNH 4 As0 4 . 6H 2 one milligram per 30 c. C. Of filtrate, and Ducru 3 adds the same amount to the weight of the anhydrous precipitate ...for each 50 c. C. Of filtrate. Dried at 100 to 102 C. , the precipitate is approxi- mately MgNH 4 As0 4 . JH 2 0, and it is not quite anhydrous at 110 C. , hence the ignition to pyroarsenate. If the ignition be conducted over a Bunsen flame, great care must be taken 1 Virgili, Zeit. F. Anal. Chem. , 44, 504.
2 Puller, Zeit. F. Anal. Chem. , 10, 53.
3 Ducru, Bull. Soc. Chim. (3), 23, 904.
122 THE ANALYSIS OF NON-FERROUS ALLOYS to exclude reducing gases. Besides covering with a lid, some workers add ammonium nitrate before commencing the ignition, which, above all, must be conducted slowly.
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To quickly assess the difficulty of the text, read a short excerpt:
1 The same end is secured by some workers by the addition of alcohol, though this might result in the pre- cipitation of magnesium salts if used too liberally. Rose recommended its addition to the extent of one-fourth the volume of the solution. Others make use of a correction for the solubility of the precipitate. Puller, 2 for example, adds to the weightf of MgNH 4 As0 4 . 6H 2 one milligram per 30 c. C. Of filtrate, and Ducru 3 adds the same amount to the weight of the anhydrous precipitate ...for each 50 c. C. Of filtrate. Dried at 100 to 102 C. , the precipitate is approxi- mately MgNH 4 As0 4 . JH 2 0, and it is not quite anhydrous at 110 C. , hence the ignition to pyroarsenate. If the ignition be conducted over a Bunsen flame, great care must be taken 1 Virgili, Zeit. F. Anal. Chem. , 44, 504.
2 Puller, Zeit. F. Anal. Chem. , 10, 53.
3 Ducru, Bull. Soc. Chim. (3), 23, 904.
122 THE ANALYSIS OF NON-FERROUS ALLOYS to exclude reducing gases. Besides covering with a lid, some workers add ammonium nitrate before commencing the ignition, which, above all, must be conducted slowly.
What to read after The Analysis of Non Ferrous Alloys?
You can find similar books in the "Read Also" column, or choose other free books by Fred Ibbotson to read onlineMoreLess
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