The Application of Victor Meyers Esterification Law to Neighboring Xylic Acid a
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9553.
Employing the Lorentz-Lorenz formula, the molecular refractivity is MV = 43. 06.
Hexahydro-2, 6-Xylic Acid. The remaining fractions from the reduction of the xylic acid together with the washings from the tetrahydro acid were freed from ether and ligroin and stirred into 20 cc. Of hydrobromic acid, saturated at 0. The mixture was covered and set away in the ice box for 24 hours. It was then let stand at room temperature for 12 hours. Crushed ice and 20 cc. Of ice-water were added and the ...solid acid separated from the solution. It was washed with cold water and suspended in sodium hydrogen carbonate solution in a flask fitted with a stirrer and surrounded with ice. A kilogram of 3% sodium amalgam was added, and carbon dioxide was passed in for 12 hours. Enough water was added from time to time to keep the bicarbonate in solution. The mercury was removed and the reduced acid thrown out with sulfuric acid. It was extracted with ether and the ether aerated off. It was then treated as before with hydrobromic acid, followed by amalgam.
What to read after The Application of Victor Meyers Esterification Law to Neighboring Xylic Acid a?
You can find similar books in the "Read Also" column, or choose other free books by Ralph William Hufferd to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
9553.
Employing the Lorentz-Lorenz formula, the molecular refractivity is MV = 43. 06.
Hexahydro-2, 6-Xylic Acid. The remaining fractions from the reduction of the xylic acid together with the washings from the tetrahydro acid were freed from ether and ligroin and stirred into 20 cc. Of hydrobromic acid, saturated at 0. The mixture was covered and set away in the ice box for 24 hours. It was then let stand at room temperature for 12 hours. Crushed ice and 20 cc. Of ice-water were added and the ...solid acid separated from the solution. It was washed with cold water and suspended in sodium hydrogen carbonate solution in a flask fitted with a stirrer and surrounded with ice. A kilogram of 3% sodium amalgam was added, and carbon dioxide was passed in for 12 hours. Enough water was added from time to time to keep the bicarbonate in solution. The mercury was removed and the reduced acid thrown out with sulfuric acid. It was extracted with ether and the ether aerated off. It was then treated as before with hydrobromic acid, followed by amalgam.
What to read after The Application of Victor Meyers Esterification Law to Neighboring Xylic Acid a?
You can find similar books in the "Read Also" column, or choose other free books by Ralph William Hufferd to read onlineMoreLess
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