The Atomic Weight of Palladium
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All weights were reduced to the vacuum standard using the following specific gravities : Pal- ladium metal, 11. 45; pallado-diammonium chloride, 2. 55; pal- lado-diammonium cyanide, 2. 5. During the course of the ex- periments the glaze on the boat gradually darkened, probably due to the absorption of minute traces of palladium. Platinum boats were tried, but it was not possible to heat them suffi- ciently high without danger of alloying. To eliminate any possible error from the absorption of p...alladium, after each experiment the boat was boiled in aqua regia and soaked in hot water. It was then dried and heated to bright redness in hydrogen for one hour. After cooling in nitrogen it was removed to the desiccator and allowed to stand in the balance room for two hours before weighing. While using this meth- od the weight of the boats did not vary more than . 03 of a milligram between any two consecutive experiments. The Reduction Apparatus. The reduction of the salt to metal was carried out in an ap- paratus which is most easily understood by means of the ac- companying sketch.
What to read after The Atomic Weight of Palladium?
You can find similar books in the "Read Also" column, or choose other free books by George Irving Kemmerer to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
All weights were reduced to the vacuum standard using the following specific gravities : Pal- ladium metal, 11. 45; pallado-diammonium chloride, 2. 55; pal- lado-diammonium cyanide, 2. 5. During the course of the ex- periments the glaze on the boat gradually darkened, probably due to the absorption of minute traces of palladium. Platinum boats were tried, but it was not possible to heat them suffi- ciently high without danger of alloying. To eliminate any possible error from the absorption of p...alladium, after each experiment the boat was boiled in aqua regia and soaked in hot water. It was then dried and heated to bright redness in hydrogen for one hour. After cooling in nitrogen it was removed to the desiccator and allowed to stand in the balance room for two hours before weighing. While using this meth- od the weight of the boats did not vary more than . 03 of a milligram between any two consecutive experiments. The Reduction Apparatus. The reduction of the salt to metal was carried out in an ap- paratus which is most easily understood by means of the ac- companying sketch.
What to read after The Atomic Weight of Palladium?
You can find similar books in the "Read Also" column, or choose other free books by George Irving Kemmerer to read onlineMoreLess
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