The Chemical And Metallographic Examination of Iron Steel And Brass
The Chemical And Metallographic Examination of Iron Steel And Brass
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Dissolve 2. 5 g. Of steel in a 300-c. C. Erlenmeyer flask with 50 c. C. Of nitric acid. Heat, and while boiling add 6 c. C. Of the strong permanganate solution, continuing to heat until manganese dioxide precipitates. Dissolve the precipitate by the addition of small portions of sodium bisulfite solution and boil until the solution is clear and free from oxides of nitrogen. Add 5 c. C. Of ammonium phosphate solution and 10 g. Of ammo- nium nitrate, heat to boiling, remove from the hot plate and... add immediately 50 c. C. Of the ammonium molybdate solution. Let stand 1 min. , then shake or agitate for 3 min. Filter the super- natant solution through an asbestos filter, washing three times with hot acid ammonium sulfate solution and drain by suction. Then place the flask containing the larger part of the precipitate under the funnel and treat the asbestos pad with successive portions of hot, concentrated sulfuric acid (d. 1. 84). Heat the solution in the flask until all the precipitate is dissolved, add a few drops of nitric acid and evaporate until copious fumes of sulfuric acid are evolved.
What to read after The Chemical And Metallographic Examination of Iron Steel And Brass?
You can find similar books in the "Read Also" column, or choose other free books by William T William Thomas Hall to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
Dissolve 2. 5 g. Of steel in a 300-c. C. Erlenmeyer flask with 50 c. C. Of nitric acid. Heat, and while boiling add 6 c. C. Of the strong permanganate solution, continuing to heat until manganese dioxide precipitates. Dissolve the precipitate by the addition of small portions of sodium bisulfite solution and boil until the solution is clear and free from oxides of nitrogen. Add 5 c. C. Of ammonium phosphate solution and 10 g. Of ammo- nium nitrate, heat to boiling, remove from the hot plate and... add immediately 50 c. C. Of the ammonium molybdate solution. Let stand 1 min. , then shake or agitate for 3 min. Filter the super- natant solution through an asbestos filter, washing three times with hot acid ammonium sulfate solution and drain by suction. Then place the flask containing the larger part of the precipitate under the funnel and treat the asbestos pad with successive portions of hot, concentrated sulfuric acid (d. 1. 84). Heat the solution in the flask until all the precipitate is dissolved, add a few drops of nitric acid and evaporate until copious fumes of sulfuric acid are evolved.
What to read after The Chemical And Metallographic Examination of Iron Steel And Brass?
You can find similar books in the "Read Also" column, or choose other free books by William T William Thomas Hall to read onlineMoreLess
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