The Chemistry And Technology of the Diazo Compounds
The Chemistry And Technology of the Diazo Compounds
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N 3, is obtained by treating aminoguanidine dinitrate with sodium nitrite in the presence of acetic acid (compare p. 128;. 5 1 Angeli, Ber. , 1893, 26, 1715; Gazzetta, 1895, 25, ii, 494.
2 Wolff, Annalen, 1912, 394, 23.
3 Prepared by treating sodium azoimide with methyl sulphate (Dimroth and Wislicenus, Ber. , 1905, 38, 1573).
4 Dimroth, Ber. , 1906, 39, 3905 ; compare ibid. , 1905, 38, 670. The first aliphatic diazoamino-compound was prepared by Thiele and Osborne, Annalen, 1899, 305, 64.
5 K.... A. Hofmann and Hock, Ber. , 1910, 43, 1866.
DIAZO-COMPOUNDS OF ALIPHATIC SERIES 131 6. Azo-compounds of the aliphatic series. Azomethane, CH, . N : N. CH 3, is prepared by oxidising s-dimethylhydrazine dihydrochloride with potassium chromate. It is a colourless gas, very readily soluble in water, solidifies a little below -78 to colourless leaflets, and boils at l-8/756 mm. 1 Other azo-compounds of the aliphatic series, as well as some azoxy-compounds, have been described.
1 Thiele, Ber. , 1909, 42, 2575.
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To quickly assess the difficulty of the text, read a short excerpt:
N 3, is obtained by treating aminoguanidine dinitrate with sodium nitrite in the presence of acetic acid (compare p. 128;. 5 1 Angeli, Ber. , 1893, 26, 1715; Gazzetta, 1895, 25, ii, 494.
2 Wolff, Annalen, 1912, 394, 23.
3 Prepared by treating sodium azoimide with methyl sulphate (Dimroth and Wislicenus, Ber. , 1905, 38, 1573).
4 Dimroth, Ber. , 1906, 39, 3905 ; compare ibid. , 1905, 38, 670. The first aliphatic diazoamino-compound was prepared by Thiele and Osborne, Annalen, 1899, 305, 64.
5 K.... A. Hofmann and Hock, Ber. , 1910, 43, 1866.
DIAZO-COMPOUNDS OF ALIPHATIC SERIES 131 6. Azo-compounds of the aliphatic series. Azomethane, CH, . N : N. CH 3, is prepared by oxidising s-dimethylhydrazine dihydrochloride with potassium chromate. It is a colourless gas, very readily soluble in water, solidifies a little below -78 to colourless leaflets, and boils at l-8/756 mm. 1 Other azo-compounds of the aliphatic series, as well as some azoxy-compounds, have been described.
1 Thiele, Ber. , 1909, 42, 2575.
What to read after The Chemistry And Technology of the Diazo Compounds?
You can find similar books in the "Read Also" column, or choose other free books by John Cannell Cain to read onlineMoreLess
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