The Gas Engineer's Laboratory Handbook

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The experiment is made as follows. About 1 gram of the carbonate (say sodium carbonate) is accurately weighed and introduced into the flask a, by the opening d. The compartment 6 is then nearly filled with dilute sulphuric acid (1 : 5), and the compartment c is half filled with strong sulphuric acid. The whole apparatus is then accurately weighed. The dilute aoid is now gradually allowed to fall into a by gently turning the stop-cook. As soon as the acid begins to act on the carbonate, bubbles
...of gas will be observed passing through the strong acid in c, and it is requisite to regulate the speed at which they pass by adjusting the rate of admission of the dilute acid, so that the separate bubbles can be easily counted. If the bubbles pass more rapidly than this, the gas will be imperfectly dried. When all the dilute acid has flowed into the flask, and bubbles of gas are no longer observed, the apparatus is plaoed upon a piece of wire gauze on an iron tripod, over a small Bunsen burner.

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