The Manufacture of Intermediate Products for Dyes
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A kinetic study of the oxidation process has been made by Bredig and Brown (Zeitsch. Physikal Chem. , 1903, 46, 502).
The following is a description of the process. (Compare H. Levinstein, J. Soc. Dyers, 1901, 17, 139, and the article on " Phthalic Acid " in Thorpe's " Dictionary of Applied Chemistry, " 1913, IV. , 250. ) In a vertical cylinder fitted with a mechanical stirrer, 350 kilos. Of naphthalene are dissolved in 3, 675 kilos, of sulphuric acid (66 Be. ) and 1, 050 kilos, of fuming sulph...uric acid (containing 23 per cent, of sulphur trioxide) by stirring for three hours.
The solution (A) so prepared is stored in a reservoir until required.
The oxidation vessel consists of an iron pan, built round with bricks and carefully heated by means of gas jets. The pan possesses a removable lid, has a flat bottom, a diameter of 6 feet, and is 2 feet deep ; a wide tube for leading off the vapours is provided, and through the top passes a shaft connected with a two-arm stirrer, worked mechanically, which just scrapes the bottom of the pan ; also several iron marbles are allowed to rotate on the pan bottom to attract charred matter, and a pressure gauge is inserted on the lid.
What to read after The Manufacture of Intermediate Products for Dyes?
You can find similar books in the "Read Also" column, or choose other free books by John Cannell Cain to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
A kinetic study of the oxidation process has been made by Bredig and Brown (Zeitsch. Physikal Chem. , 1903, 46, 502).
The following is a description of the process. (Compare H. Levinstein, J. Soc. Dyers, 1901, 17, 139, and the article on " Phthalic Acid " in Thorpe's " Dictionary of Applied Chemistry, " 1913, IV. , 250. ) In a vertical cylinder fitted with a mechanical stirrer, 350 kilos. Of naphthalene are dissolved in 3, 675 kilos, of sulphuric acid (66 Be. ) and 1, 050 kilos, of fuming sulph...uric acid (containing 23 per cent, of sulphur trioxide) by stirring for three hours.
The solution (A) so prepared is stored in a reservoir until required.
The oxidation vessel consists of an iron pan, built round with bricks and carefully heated by means of gas jets. The pan possesses a removable lid, has a flat bottom, a diameter of 6 feet, and is 2 feet deep ; a wide tube for leading off the vapours is provided, and through the top passes a shaft connected with a two-arm stirrer, worked mechanically, which just scrapes the bottom of the pan ; also several iron marbles are allowed to rotate on the pan bottom to attract charred matter, and a pressure gauge is inserted on the lid.
What to read after The Manufacture of Intermediate Products for Dyes?
You can find similar books in the "Read Also" column, or choose other free books by John Cannell Cain to read onlineMoreLess
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