The Manufacture of Salicylic Acid

Cover The Manufacture of Salicylic Acid
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As it was desirable to use if possible this ■autoclave, of wnich there were several on hand being used for another purpose, it was decided to add a stirring devise which should keep tne saltin notion, and thus prevent Its packing down. Carrying out this idea, a new cover was made carrying a stirring mechanism as shown m Pig. 2* the thermometer well Pi^. 2.
beinf? snifted to coaie bstween the two vertical slats and deep enoudb to just clear tne upper Uoriaontal one. Toe sodiuoi pQenate as before
... was put in taru tfte ftaod nole until toe stirrer slats were just covered. Tne run was made until no more gas seeiDed to be absorbed and toe salt removed in tnree layers (smaller portions were too difficult to get out on account of tne slats). Tne upper layer was well converted, toe middle layer to tne extent of 89%, and tne lower layer «nicn *as well powdered by tne stirring action, to the extent of 18%. In another trial it was found impossible to raise tnis percentage in the lower layer more tnan •1% by doubling the gassing time.

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