The Organic Chemistry of Nitrogen
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Or the diazo-group may be replaced by iodine, and the product reduced, for example, by distillation over zinc dust. A reaction which is often used for this purpose is Friedlander's. This consists in treating the diazo-salt with an alkaline stannous solution. It has been shown 3 that in this reaction part of the salt is reduced to the hydrazine, which is then oxidized by the rest of the diazo- compound to the hydrocarbon.
4. Halogens. This is effected in various ways : sometimes by heating with ...excess of hydrochloric or hydrobromic acid, or by heating the platinichloride with soda.
The best method is that of Sandmeyer, 4 which consists in heating the chloride or bromide in presence of cuprous chloride or bromide : Ar-N 2 . Br = Ar-Br + N 2 .
1 Remsen, Palmer, Am. Ch. J. 8. 243 (1886) ; Remsen, Dashiell, ib. 15. 105 (1893).
2 Remsen, Palmer, 1. C. ; Cameron, ib. 2O. 229 (1898). 3 Eibner, Bet: 36. 813. 4 Ber. 17. 1633, 2650 (1884).
Reactions of Diazo-compounds 261 The diazo-solution is usually added to the cuprous solution, which has been warmed to a suitable temperature.
What to read after The Organic Chemistry of Nitrogen?
You can find similar books in the "Read Also" column, or choose other free books by Nevil Vincent Sidgwick to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
Or the diazo-group may be replaced by iodine, and the product reduced, for example, by distillation over zinc dust. A reaction which is often used for this purpose is Friedlander's. This consists in treating the diazo-salt with an alkaline stannous solution. It has been shown 3 that in this reaction part of the salt is reduced to the hydrazine, which is then oxidized by the rest of the diazo- compound to the hydrocarbon.
4. Halogens. This is effected in various ways : sometimes by heating with ...excess of hydrochloric or hydrobromic acid, or by heating the platinichloride with soda.
The best method is that of Sandmeyer, 4 which consists in heating the chloride or bromide in presence of cuprous chloride or bromide : Ar-N 2 . Br = Ar-Br + N 2 .
1 Remsen, Palmer, Am. Ch. J. 8. 243 (1886) ; Remsen, Dashiell, ib. 15. 105 (1893).
2 Remsen, Palmer, 1. C. ; Cameron, ib. 2O. 229 (1898). 3 Eibner, Bet: 36. 813. 4 Ber. 17. 1633, 2650 (1884).
Reactions of Diazo-compounds 261 The diazo-solution is usually added to the cuprous solution, which has been warmed to a suitable temperature.
What to read after The Organic Chemistry of Nitrogen?
You can find similar books in the "Read Also" column, or choose other free books by Nevil Vincent Sidgwick to read onlineMoreLess
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