The Preparation of Benzoic Acid By Oxidation of Toluol
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This Y/ould have heen the most su.itahle pointfor a pressure gauge, "but it was not found convenient to insert one.
In mailing the runs, a measured arnou.nt of acid was pi ced in the box, and the box wa- then supported on a water bath. The cover was placed on the box and all craclis were stopped v/ith the BaSO^, , asbestos water-glass mixture. The cover was held in place b" suitable clamps. T"^e tem- perature in the box v;as raised to 85 0., and then the toluene wa^^ heated. The toluene vapor t...hen passed over into the acid mixture. The valve between the box and condenser v/as closed.
15.
Oxidation of Toluol to Benzoic Icid In the first run tlie toluene came through quite vigorously, "but the distrihution v/as not v;hat v/as desired. l.Iost of the vapor escaped through the first fev/ holes. In the second run this was corrected "by sealing these holes v/ith water-glass. In this latter run the distrihu- tion was very satisfactory. Considerable toluene vapor was ohserved ahove the acid surface.
What to read after The Preparation of Benzoic Acid By Oxidation of Toluol?
You can find similar books in the "Read Also" column, or choose other free books by Grigsby, D. W to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
This Y/ould have heen the most su.itahle pointfor a pressure gauge, "but it was not found convenient to insert one.
In mailing the runs, a measured arnou.nt of acid was pi ced in the box, and the box wa- then supported on a water bath. The cover was placed on the box and all craclis were stopped v/ith the BaSO^, , asbestos water-glass mixture. The cover was held in place b" suitable clamps. T"^e tem- perature in the box v;as raised to 85 0., and then the toluene wa^^ heated. The toluene vapor t...hen passed over into the acid mixture. The valve between the box and condenser v/as closed.
15.
Oxidation of Toluol to Benzoic Icid In the first run tlie toluene came through quite vigorously, "but the distrihution v/as not v;hat v/as desired. l.Iost of the vapor escaped through the first fev/ holes. In the second run this was corrected "by sealing these holes v/ith water-glass. In this latter run the distrihu- tion was very satisfactory. Considerable toluene vapor was ohserved ahove the acid surface.
What to read after The Preparation of Benzoic Acid By Oxidation of Toluol?
You can find similar books in the "Read Also" column, or choose other free books by Grigsby, D. W to read onlineMoreLess
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