The Preparation of Salicylic Aldehyde
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The rise of the "boiling point as heat was applied to the mixture of o-cresol and phosphorus-oxy-chloride and the time it required for the two substances to come to a constant boiling point are shown in the following table.
TABLE 1-A.
Time ir I Minutes' Temperature in 00, 20 10 65 20 86 30 94 40 105 50 113 60 (Ihr) 122 70 135 30 143 90 155 100 165 110 169 120 (Shrs) 173 130 180 140 187 150 194 160 193 170 195 180 (3hrs) 197 190 197 200 203 210 207 &RAPH TABLE la.
/ / / 1 1 r-r-Qr- 1 ; .;: ._, M...fNU TL M£ IK/ T£ S 32.
Time in Minutes Temperature in OC 220 206 230 205 240 (4hrs) 204 250 204 260 205 270 207 280 206 290 205 300 (Shrs) 206 310 206 320 206 330 . 206 The reaction of the o-cresol and phosphorus-osQrr-'chlorids protably takes place as shown m the following equation: OH ^—CH, \ "^J -^-POCIj = ^Z2>°~~/^"^ ^~~r//.
?//3 A tube was then inserted in the stopper and run to the bottom of the flask so that a stream of chlorine gas could be passed through the liquid. The temperature of the liquid was kept betv/een 1600«i80oc».
What to read after The Preparation of Salicylic Aldehyde?
You can find similar books in the "Read Also" column, or choose other free books by Clarke C. B. to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
The rise of the "boiling point as heat was applied to the mixture of o-cresol and phosphorus-oxy-chloride and the time it required for the two substances to come to a constant boiling point are shown in the following table.
TABLE 1-A.
Time ir I Minutes' Temperature in 00, 20 10 65 20 86 30 94 40 105 50 113 60 (Ihr) 122 70 135 30 143 90 155 100 165 110 169 120 (Shrs) 173 130 180 140 187 150 194 160 193 170 195 180 (3hrs) 197 190 197 200 203 210 207 &RAPH TABLE la.
/ / / 1 1 r-r-Qr- 1 ; .;: ._, M...fNU TL M£ IK/ T£ S 32.
Time in Minutes Temperature in OC 220 206 230 205 240 (4hrs) 204 250 204 260 205 270 207 280 206 290 205 300 (Shrs) 206 310 206 320 206 330 . 206 The reaction of the o-cresol and phosphorus-osQrr-'chlorids protably takes place as shown m the following equation: OH ^—CH, \ "^J -^-POCIj = ^Z2>°~~/^"^ ^~~r//.
?//3 A tube was then inserted in the stopper and run to the bottom of the flask so that a stream of chlorine gas could be passed through the liquid. The temperature of the liquid was kept betv/een 1600«i80oc».
What to read after The Preparation of Salicylic Aldehyde?
You can find similar books in the "Read Also" column, or choose other free books by Clarke C. B. to read onlineMoreLess
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