The Production of Metol
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Platinum electrodes Cur. Den. 5 to 6 amps./ sq. dm.
Temperature 75 to 80°G.
E. K. F. 7.4 volts. 7.0 volts.
Porous pot diaphragm used.
Yield 14;2 16;^ Yie made two runs on the chemical reduction of nitrobenzene in neutral solution using pov/- dered zinc as a reductor. In both cases the yield was below 12)3. A good discussion of the possibilities of reduction in neutral solutions is given in the article by P. Li. Fredericksen previously i^entioned.
The methylatlon of para aminophenol is ac- compl...ished by heating the hydrochloride of para aminophenol with methyl alcohol to ISO to 200° C. for a period of 6 to 8 hours.
15 It may better be accoiapllshed by heating in a similar way v.'ith methyl chloride. In either' case the tendency is for tiie formation of the di- methyl body and if the theoretical quantities are used, a large amount of the di:aethyl body is formed and much of the para aminophenol re- mains unattacked. This reaction was not stud- ied but the general trend of information from different sources seems to corroborate these statements .
What to read after The Production of Metol?
You can find similar books in the "Read Also" column, or choose other free books by Smith, A. H to read onlineMoreLess
To quickly assess the difficulty of the text, read a short excerpt:
Platinum electrodes Cur. Den. 5 to 6 amps./ sq. dm.
Temperature 75 to 80°G.
E. K. F. 7.4 volts. 7.0 volts.
Porous pot diaphragm used.
Yield 14;2 16;^ Yie made two runs on the chemical reduction of nitrobenzene in neutral solution using pov/- dered zinc as a reductor. In both cases the yield was below 12)3. A good discussion of the possibilities of reduction in neutral solutions is given in the article by P. Li. Fredericksen previously i^entioned.
The methylatlon of para aminophenol is ac- compl...ished by heating the hydrochloride of para aminophenol with methyl alcohol to ISO to 200° C. for a period of 6 to 8 hours.
15 It may better be accoiapllshed by heating in a similar way v.'ith methyl chloride. In either' case the tendency is for tiie formation of the di- methyl body and if the theoretical quantities are used, a large amount of the di:aethyl body is formed and much of the para aminophenol re- mains unattacked. This reaction was not stud- ied but the general trend of information from different sources seems to corroborate these statements .
What to read after The Production of Metol?
You can find similar books in the "Read Also" column, or choose other free books by Smith, A. H to read onlineMoreLess
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