The Study of the Formation of Chromates

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17.80 57.50 -18- Cliarge Ho. 4» Finding that the amount of sodium chromate decreased with the increase in the amount of so- dium cartonate, it was decided to make this run with less of the soda ash. That amount used is the theoretical alkali equivalent, independent of the caustic soda. The analysis was: Ctj^Oj 1 Ih.
22.95S HaOH 2 Ih.
39.9^ Bag 00^ 1.38 Ih.
29.6^ In order that the results would "be compara- tive, it was decided that the temperature should he as near constant as possible for all
...the runs, This temperature happened to fall hetween 435 * and 475* C.
In this run, the temperature at the start was 275" , rising to a temperature of 465 '^ at the end of the first half hour, and remaining at the average temperature of 455* for the remaining part of the run.
-19- ^^ r^ IJ^^^P »« . •.-.• •■■ •\y,,i.iK>'( c ..•v-rr.Br'ii ii»ul«v.i.lrs«j|*-iit ..'Litis.'. .' " 'f , %jiw»«ti: ■■«« •■■'.i-ij.x » n ■ • v ■!..-'. ••'*'*•.
o The amount of sodium chr ornate formed in- creased hourly and reached a maximum at the end of the run, which was four hours after we had started, ITo doubt this run should have teen at least one and one half hours longer; however, the results are indicative of what may have happened in a long- er run.


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