Water Gas And Its Residue

Cover Water Gas And Its Residue
Water Gas And Its Residue
John Campbell Godbey
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61%. 500 cc. Of fraction I. Was dried with calcium chlo- ride and refractionated, using the hempel three-bulb tube and completing each fraction as in the distillations on a small scale. Fraction Range in Temp. Amt. In C. 'C. 1. 60 100C 65 2. 100 120C 93 3. 120 160'C 184 Residue above 160 C 158 These fractions were again refractionated, giving the following results: Fraction 1 : Fraction Range in Temp. Amt. In C. C. A. 60 80C 2 b. 80' 85C 27. 5 c. 85 100C 20 Above 100>C 15. 5 Mourn. Chem. Soc. ,... Vol. LIX. , pp. 605 and 1090; Treatise on Chem. , Roscoe and Schorlmner, p. 1019. Mourn. 'Chem. Soc. , Vol. LIX. , p. 1093. 37 Fraction 2-1- residue from 1. A. 85 100 C 35 b. 100 105C 10 c. 105 115C 40 d. 115 120C 22 Above 120C 1. 5 Fraction 34- residue from 2. A. 120 130C 57. 5 b. 130 150'C 83 c. 150 160C 10 Above 160C 32 Fractions la and Ib were tested for carbon bisul- phide according to the method devised by Nickels. 1 A portion of the distillate was treated with a solution of potassium hydroxide in absolute alcohol (1 g.

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